5.1 This test method is one of a number of tests conducted on heavy hydrocarbon mixtures to characterize these materials for a refiner or a purchaser. It provides an estimate of the yields of fractions of various boiling ranges.
5.2 The fractions made by this test method can be used alone or in combination with other fractions to produce samples for analytical studies and quality evaluations.
5.3 Residues to be used in the manufacture of asphalt can also be made but may not always be suitable. The long heat soaking that occurs in this test method may alter some of the properties.
5.5 This is a complex procedure involving many interacting variables. It is most important that at the time of first use of a new apparatus, its components be checked as detailed in Annex A1 and Annex A2 and that the location of the vapor temperature sensor be verified as detailed in 6.5.3 and Fig. 1.
1.1 This test method covers the procedure for distillation of heavy hydrocarbon mixtures having initial boiling points greater than 150°C (300°F), such as heavy crude oils, petroleum distillates, residues, and synthetic mixtures. It employs a potstill with a low pressure drop entrainment separator operated under total takeoff conditions. Distillation conditions and equipment performance criteria are specified and typical apparatus is illustrated.
1.2 This test method details the procedures for the production of distillate fractions of standardized quality in the gas oil and lubricating oil range as well as the production of standard residue. In addition, it provides for the determination of standard distillation curves to the highest atmospheric equivalent temperature possible by conventional distillation.
1.3 The maximum achievable atmospheric equivalent temperature (AET) is dependent upon the heat tolerance of the charge. For most samples, a temperature up to 565°C (1050°F) can be attained. This maximum will be significantly lower for heat sensitive samples (for example, heavy residues) and might be somewhat higher for nonheat sensitive samples.
1.4 The recommended distillation method for crude oils up to cutpoint 400°C (752°F) AET is Test Method D2892. This test method can be used for heavy crude oils with initial boiling points greater than 150°C (302°F). However, distillation curves and fraction qualitie......
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