ASTM D5236-01
Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)

Standard No.
ASTM D5236-01
Release Date
2001
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D5236-02
Latest
ASTM D5236-23
Scope

1.1 This test method covers the procedure for distillation of heavy hydrocarbon mixtures having initial boiling points greater than 150176;C (300176;F), such as heavy crude oils, petroleum distillates, residues, and synthetic mixtures. It employs a potstill with a low pressure drop entrainment separator operated under total takeoff conditions. Distillation conditions and equipment performance criteria are specified and typical apparatus is illustrated.

1.2 This test method details the procedures for the production of distillate fractions of standardized quality in the gas oil and lubricating oil range as well as the production of standard residua. In addition, it provides for the determination of standard distillation curves to the highest atmospheric equivalent temperature possible by conventional distillation.

1.3 The maximum achievable atmospheric equivalent temperature (AET) is dependent upon the heat tolerance of the charge. For most samples, a temperature up to 565176;C (10570176;F) can be attained. This maximum will be significantly lower for heat sensitive samples (for example, heavy residues) and might be somewhat higher for nonheat sensitive samples.

1.4 The recommended distillation method for crude oils up to cutpoint 400176;C (752176;F) AET is Test Method D 2892. This test method can be used for heavy crude oils with initial boiling points greater than 1508212;C (302176;F). However, distillation curves and fraction qualities obtained by these methods are not comparable.

1.5 This test method contains the following annexes:

1.5.1 Annex A18212;Test Method for Determination of the Temperature Response Time,

1.5.2 Annex A28212;Practice for Calibration of Sensors,

1.5.3 Annex A38212;Test Method for Dehydration of a Wet Sample of Oil,

1.5.4 Annex A48212;Practice for Conversion of Observed Vapor Temperature to Atmospheric Equivalent Temperature (AET), and

1.5.5 Annex A58212;Test Method for Determination of Wettage.

1.6 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are provided for information purposes only.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warnings see 6.5.4.2, 6.5.6.3, 6.9.3, 9.5, 9.6 and A2.3.1.3.

ASTM D5236-01 history

  • 2023 ASTM D5236-23 Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2018 ASTM D5236-18a Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2018 ASTM D5236-18 Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2017 ASTM D5236-17 Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2013 ASTM D5236-13 Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2003 ASTM D5236-03(2011) Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2003 ASTM D5236-03(2007) Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2003 ASTM D5236-03 Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2002 ASTM D5236-02 Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 2001 ASTM D5236-01 Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)
  • 1999 ASTM D5236-99ae1 Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)



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