EN 16693:2015
Water quality - Determination of organochlorine pesticides (OCP) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)

Standard No.
EN 16693:2015
Release Date
2015
Published By
European Committee for Standardization (CEN)
Latest
EN 16693:2015
Replace
FprEN 16693-2015
Scope
This European Standard specifies a method for the determination of selected organochlorine pesticides (OCP), in water samples. The method uses solid-phase extraction with SPE-disks followed by gas chromatography-mass spectrometry (GC-MS). It is applicable to the analysis of OCPs in surface water containing suspended particulate matter (SPM) up to 500 mg/l (whole water samples), drinking water and groundwater. The lower limit of the working range depends on the matrix, on the specific compound to be analyzed and on the sensitivity of the mass spectrometric detection unit. For compounds listed in Table 1 the limit of determination (LOQ) is at least 30 % of the corresponding AA- EQS value (0,000 15 µg/l to 0,1 µg/l) according to the requirements of the European Quality Standards Directive (Directive 2008/105/EC) for both inland surface waters and other surface waters. This method may be used for the analysis of other OCPs not listed in Table 1 or other types of water. However, it is important to verify its applicability before use.

EN 16693:2015 Referenced Document

  • EN ISO 22892:2011 Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
  • EN ISO 3696:1995 Water for Analytical Laboratory Use- Specification and Test Methods (ISO 3696 : 1987)
  • EN ISO 5667-1:2006 Water quality - Sampling - Part 1: Guidance on the design of sampling programmes and sampling techniques (Incorporating corrigendum March 2007)*2024-04-20 Update
  • EN ISO 5667-3:2012 Water quality - Sampling - Part 3: Preservation and handling of water samples*2024-04-20 Update
  • ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
  • ISO 8466-1:1990 Water quality; calibration and evaluation of analytical methods and estimation of performance characteristics; part 1: statistical evaluation of the linear calibration function
  • ISO/TS 28581:2012 Water quality - Determination of selected non-polar substances - Method using gas chromatography with mass spectrometric detection (GC-MS)

EN 16693:2015 history

  • 2015 EN 16693:2015 Water quality - Determination of organochlorine pesticides (OCP) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)



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