EN 16877:2016 Animal feeding stuffs: Methods of sampling and analysis - Determination of T-2 and HT-2 toxins@ Deoxynivalenol and Zearalenone@ in feed materials and compound feed by LCMS
This method of analysis is applicable to the determination of HT-2 toxin (HT2) in the tested range of 22 µg/kg to 178 µg/kg, T-2 toxin (T2) in the tested range of 7 µg/kg to 50 µg/kg, Deoxynivalenol (DON) in the tested range of 88 µg/kg to 559 µg/kg, and Zearalenone (ZON) in the tested range of 14 µg/kg to 430 µg/kg in cereals and cereal-based compound animal feed. The actual working ranges may extend beyond the tested ranges. It is the responsibility of the laboratory to prove that the limit of quantitation (LOQ) for HT-2 and T-2 toxin is 10 µg/kg, for DON 100 µg/kg, and for ZON 20µg/kg.
EN 16877:2016 Referenced Document
EN ISO 3696:1995 Water for Analytical Laboratory Use- Specification and Test Methods (ISO 3696 : 1987)
EN ISO 6498:2012 Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 5725-5:1998 Accuracy (trueness and precision) of measurement methods and results - Part 5: Alternative methods for the determination of the precision of a standard measurement method
EN 16877:2016 history
2016EN 16877:2016 Animal feeding stuffs: Methods of sampling and analysis - Determination of T-2 and HT-2 toxins@ Deoxynivalenol and Zearalenone@ in feed materials and compound feed by LCMS