ASTM D7823-16
Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly (Vinyl Chloride) Plastics by Thermal Desorption&x2014;Gas Chromatography/Mass Spectrometry

Standard No.
ASTM D7823-16
Release Date
2016
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D7823-18
Latest
ASTM D7823-20
Scope

5.1 Identification and quantitation of phthalates: DBP, BBP, DEHP, DNOP, DINP, and DIDP are required for regulated articles. Regulations include: EU—Directive 2005/84/EC, US—Consumer Product Safety Improvement Act of 2008—section 108, Japan—Health, Labor and Welfare Ministry guideline No.336 (2010). This test method provides a procedure to identify and quantify regulated phthalates in PVC.

5.2 Other techniques successfully used to separate and identify phthalates in PVC include GC/MS, HPLC/UV, HPLC/MS, FTIR, and GC/FID (flame ionization detector).

1.1 This test method provides a procedure to identify and quantify six phthalates by thermal desorption (TD) gas chromatography (GC) mass spectrometry (MS). The phthalates are BBP, DBP, DEHP, DNOP, DINP and DIDP.

Note 1: The method can be extended to include other phthalates.

1.2 Within the context of this method, “low level” is defined as 1000 ppm.

1.3 The values in SI units are to be regarded as standard.

1.4 This test method includes references, notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in the tables and figures) shall not be considered as requirements of this method.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Note 2: There is no known ISO equivalent to this standard.

ASTM D7823-16 Referenced Document

  • ASTM D1600 Standard Terminology for Abbreviated Terms Relating to Plastics
  • ASTM D3465 Standard Guide for Purity of Monomeric Plasticizers by Gas Chromatography
  • ASTM D7083 Standard Practice for Determination of Monomeric Plasticizers in Poly (Vinyl Chloride) (PVC) by Gas Chromatography
  • ASTM D883 Standard Terminology Relating to Plastics
  • ASTM E177 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
  • ASTM E355 Standard Practice for Gas Chromatography Terms and Relationships*2024-04-20 Update
  • ASTM E594 Standard Practice for Testing Flame Ionization Detectors Used in Gas or Supercritical Fluid Chromatography
  • ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

ASTM D7823-16 history

  • 2020 ASTM D7823-20 Standard Test Method for Determination of Low Level Phthalates in Poly (Vinyl Chloride) Plastics by Thermal Desorption—Gas Chromatography/Mass Spectrometry
  • 2018 ASTM D7823-18 Standard Test Method for Determination of Low Level Phthalates in Poly (Vinyl Chloride) Plastics by Thermal Desorption—Gas Chromatography/Mass Spectrometry
  • 2016 ASTM D7823-16 Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly (Vinyl Chloride) Plastics by Thermal Desorption&x2014;Gas Chromatography/Mass Spectrometry
  • 2014 ASTM D7823-14 Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly &40;Vinyl Chloride&41; Plastics by Thermal Desorption—Gas Chromatography/Mass Spectrometry
  • 2013 ASTM D7823-13 Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly (Vinyl Chloride) Plastics by Thermal Desorptionmdash;Gas Chromatography/Mass Chromatography
Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly (Vinyl  Chloride) Plastics by Thermal Desorption&x2014;Gas Chromatography/Mass  Spectrometry



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