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ASTM D5666-95(2014)
Standard Test Method for Rubber Chemical Antidegradants—Purity of p -Phenylenediamine (PPD) Antidegradants by High Performance Liquid Chromatography

Standard No.
ASTM D5666-95(2014)
Release Date
1995
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D5666-95(2019)
Latest
ASTM D5666-95(2023)
Scope

5.1 This test method is designed to determine the purity of p-phenylenediamine antidegradants.

5.2 Since the results of this test method are based on an integrated peak area as determined by HPLC, it is assumed that all analytes of interest are resolved from interfering peaks.

1.1 This test method covers the purity of Type I, II, and III p-phenylenediamine (PPD) antidegradants as described in Classification D4676 by high performance liquid chromatography (HPLC) using ultraviolet detection and external standard calculations.

1.2 Expertise in HPLC is necessary to the successful application of this test method.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D5666-95(2014) Referenced Document

  • ASTM D3853 Standard Terminology Relating to Rubber and Rubber Latices-Abbreviations for Chemicals Used in Compounding*1997-04-20 Update
  • ASTM D4483 Standard Practice for Determining Precision for Test Method Standards in the Rubber and Carbon Black Industries*1999-04-20 Update
  • ASTM D4676 Standard Classification for Rubber Compounding Materials—Antidegradants*2021-11-01 Update
  • ISO 5725 Precision of test methods; Determination of repeatability and reproducibility for a standard test method by inter-laboratory tests
  • ISO 6472 Rubber compounding ingredients - Abbreviated terms*2017-06-01 Update

ASTM D5666-95(2014) history

  • 2023 ASTM D5666-95(2023) Standard Test Method for Rubber Chemical Antidegradants—Purity of p-Phenylenediamine (PPD) Antidegradants by High Performance Liquid Chromatography
  • 2019 ASTM D5666-95(2019) Standard Test Method for Rubber Chemical Antidegradants—Purity of p-Phenylenediamine (PPD) Antidegradants by High Performance Liquid Chromatography
  • 1995 ASTM D5666-95(2014) Standard Test Method for Rubber Chemical Antidegradants—Purity of p -Phenylenediamine (PPD) Antidegradants by High Performance Liquid Chromatography
  • 1995 ASTM D5666-95(2009) Standard Test Method for P-Phenylenediamine Antidegradants-Purity by High Performance Liquid Chromatography
  • 1995 ASTM D5666-95(2004)e1 Standard Test Method for P-Phenylenediamine Antidegradants-Purity by High Performance Liquid Chromatography
  • 1995 ASTM D5666-95(2000) Standard Test Method for P-Phenylenediamine Antidegradants-Purity by High Performance Liquid Chromatography
Standard Test Method for  Rubber Chemical Antidegradants—Purity of <emph type="bdit"  >p </emph>-Phenylenediamine (PPD) Antidegradants by High Performance  Liquid Chromatography



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