ASTM D1065-96(2014)e1
Standard Test Method for Unsaponifiable Matter in Naval Stores, Including Rosin, Tall Oil, and Related Products
- Standard No.
- ASTM D1065-96(2014)e1
- Release Date
- 1996
- Published By
- American Society for Testing and Materials (ASTM)
- Status
- Replace By
- ASTM D1065-18
- Latest
- ASTM D1065-18(2022)
- Scope
3.1 This test method is designed to broaden the scope of the previous edition of the test method by the inclusion of tall oil and tall oil derived from products as test materials. Test Methods D803 currently includes a method for the determination of unsaponifiable matter.
div class="SectionLevel2">3.2 The amount of unsaponifiable matter in tall oil and other related products is important in characterizing such products as it indicates the level of nonacidic material, both free and combined, present in the test material. The unsaponifiable in naval stores products is primarily composed of higher molecular weight alcohols, sterols, and hydrocarbons.
1.1 This test method covers the determination of the percentage of material in Naval Stores products as defined in Terminology D804 including rosin, tall oil and related products, other than insoluble dirt or similar visible foreign matter that does not yield a water-soluble soap when the sample is saponified with potassium hydroxide.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1: It has been reported that this method may not be applicable to gum rosin, especially any gum rosin containing volatile terpenes. Volatile terpenes are by definition unsaponifiable matter, and can be lost under the drying conditions described in 8.4. The method is applicable to tall oil rosin and wood rosin as these rosins do not contain volatile terpenes.
ASTM D1065-96(2014)e1 Referenced Document
- ASTM D509 Standard Test Methods of Sampling and Grading Rosin*， 1998-04-20 Update
- ASTM D803 Standard Test Methods for Testing Tall Oil*， 1997-04-20 Update
- ASTM D804 Terminology Relating to Naval Stores, Including Tall Oil and Related Products*， 1997-04-20 Update
- ASTM E177 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
- ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method*， 1999-04-20 Update
ASTM D1065-96(2014)e1 history
- 2022 ASTM D1065-18(2022) Standard Test Method for Unsaponifiable Matter in Pine Chemicals, Including Rosin, Tall Oil, and Related Products
- 2018 ASTM D1065-18 Standard Test Method for Unsaponifiable Matter in Pine Chemicals, Including Rosin, Tall Oil, and Related Products
- 1996 ASTM D1065-96(2014)e1 Standard Test Method for Unsaponifiable Matter in Naval Stores, Including Rosin, Tall Oil, and Related Products
- 1996 ASTM D1065-96(2010) Standard Test Method for Unsaponifiable Matter in Naval Stores, Including Rosin, Tall Oil, and Related Products
- 1996 ASTM D1065-96(2006) Standard Test Method for Unsaponifiable Matter in Naval Stores, Including Rosin, Tall Oil, and Related Products
- 1996 ASTM D1065-96(2001) Standard Test Method for Unsaponifiable Matter in Naval Stores, Including Rosin, Tall Oil, and Related Products
- 2001 ASTM D1065-96 Standard Test Method for Unsaponifiable Matter in Naval Stores, Including Rosin, Tall Oil, and Related Products
