ASTM D3321-13
Standard Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants

Standard No.

ASTM D3321-13

Release Date

2013

Published By

American Society for Testing and Materials (ASTM)

Status

Be replaced

Replace By

ASTM D3321-19

Latest

ASTM D3321-19(2023)

Scope

4.1 This practice is commonly used by vehicle service personnel to determine the freezing point, in degrees Celsius or Fahrenheit, of aqueous solutions of commercial ethylene and propylene glycol-based coolant. A durable hand-held refractometer is available that reads the freezing point, directly, in degrees Celsius or Fahrenheit, when a few drops of engine coolant are properly placed on the temperature-compensated prism surface of the refractometer. This refractometer is for glycol and water solutions, and is not suitable for other coolant solutions.

4.2 The hand-held refractometer should be calibrated before use (see Section 7).

4.3 Care must be taken to use the correct glycol freezing point scale for the glycol type being measured. Use of the wrong glycol scale can result in freezing point errors of 18 and more degrees Fahrenheit.

4.4 Ethylene glycol/propylene glycol mixtures will result in inaccurate freezing point measurements using either freezing point scale.

1.1 This test method covers the use of a portable refractometer for determining the approximate freezing protection provided by ethylene and propylene glycol-based coolant solutions as used in engine cooling systems and special applications.

Note 1—Some instruments have a supplementary freezing protection scale for methoxypropanol coolants. Others carry a supplemental scale calibrated in density or specific gravity readings of sulfuric acid solutions so that the refractometer can be used to determine the charged condition of lead acid storage batteries.

1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D3321-13 history

• 2023 ASTM D3321-19(2023) Standard Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants
• 2019 ASTM D3321-19 Standard Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants
• 2013 ASTM D3321-13 Standard Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants
• 2012 ASTM D3321-12 Standard Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants
• 2007 ASTM D3321-94(2007) Standard Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants
• 1994 ASTM D3321-94(2002) Standard Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants
• 1998 ASTM D3321-94(1998) Standard Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants