This method is suitable for the determination of ammonium in drinking water and wastewater. Using a 10m1 test portion, the ammonium nitrogen content in the test portion can be determined up to 10 mg, which is equivalent to a sample concentration of up to 1000 mg/L. The minimum detection concentration uses a 250ml test portion, and the minimum detection concentration actually measured (degrees of freedom is 4) is 0.2mg/L of nitrogen. Sensitivity Use 100ml test portion, 1.0m10.02mol/L hydrochloric acid is equivalent to 2.8mg/L nitrogen. Interfering urea may be the main interference, which distills out as ammonia under the specified conditions, causing high results, as well as volatile amines, which are distilled off and react with acids during titration, thus giving high results. Chloramines present in chlorinated samples are also determined in this way.
GB/T 7478-1987 history
1987GB/T 7478-1987 Water quality--Determination of ammonium--Distillation and titration method
GB/T 7478-1987 Water quality--Determination of ammonium--Distillation and titration method was changed to HJ 537-2009 Water quality.Determination of ammonia nitrogen.Distillation-neutralization titration.