ASTM C1359-11
Standard Test Method for Monotonic Tensile Strength Testing of Continuous Fiber-Reinforced Advanced Ceramics With Solid Rectangular Cross-Section Test Specimens at Elevated Temperatures

Standard No.
ASTM C1359-11
Release Date
2011
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM C1359-13
Latest
ASTM C1359-18e1
Scope

This test method may be used for material development, material comparison, quality assurance, characterization, reliability assessment, and design data generation.

Continuous fiber-reinforced ceramic matrix composites generally characterized by crystalline matrices and ceramic fiber reinforcements are candidate materials for structural applications requiring high degrees of wear and corrosion resistance, and elevated-temperature inherent damage tolerance (that is, toughness). In addition, continuous fiber-reinforced glass (amorphous) matrix composites are candidate materials for similar but possibly less-demanding applications. Although flexural test methods are commonly used to evaluate strengths of monolithic advanced ceramics, the non-uniform stress distribution of the flexure test specimen in addition to dissimilar mechanical behavior in tension and compression for CFCCs leads to ambiguity of interpretation of strength results obtained from flexure tests for CFCCs. Uniaxially-loaded tensile-strength tests provide information on mechanical behavior and strength for a uniformly stressed material.

Unlike monolithic advanced ceramics that fracture catastrophically from a single dominant flaw, CFCCs generally experience graceful'' (that is, non-catastrophic, ductile-like stress-strain behavior) fracture from a cumulative damage process. Therefore, the volume of material subjected to a uniform tensile stress for a single uniaxially-loaded tensile test may not be as significant a factor in determining the ultimate strengths of CFCCs. However, the need to test a statistically significant number of tensile test specimens is not obviated. Therefore, because of the probabilistic nature of the strengths of the brittle fibers and matrices of CFCCs, a sufficient number of test specimens at each testing condition is required for statistical analysis and design. Studies to determine the influence of test specimen volume or surface area on strength distributions for CFCCs have not been completed. It should be noted that tensile strengths obtained using different recommended tensile test specimen geometries with different volumes of material in the gage sections may be different due to these volume differences.

Tensile tests provide information on the strength and deformation of materials under uniaxial tensile stresses. Uniform stress states are required to effectively evaluate any non-linear stress-strain behavior that may develop as the result of cumulative damage processes (for example, matrix cracking, matrix/fiber debonding, fiber fracture, delamination, and so forth) that may be influenced by testing mode, testing rate, effects of processing or combinations of constituent materials, environmental influences, or elevated temperatures. Some of these effects may be consequences of stress corrosion or sub critical (slow) crack growth that can be minimized by testing at sufficiently rapid rates as outlined in this test method.

The results of tensile tests of test specimens fabricated to standardized dimensions from a particular material or selected portions of a part, or both, may not totally represent the strength and deformation properties of the entire, full-size end product or its in-service behavior in different environments or various elevated temperatures.

For quality control purposes, results derived from standardized tensile test specimens may be considered indicative of the response of the material from which they were taken for the particular primary processing conditions and post-processing heat treatments.

The tensile behavior and strength of a CFCC are dependent on its inherent resistance to fracture, the presence of flaws, or damage accumulation processes, or both. Analysis of fracture surfaces and fractography, though beyond the scope of this test method, is recommended.