ASTM C799-99(2005)
Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Uranyl Nitrate Solutions

Standard No.
ASTM C799-99(2005)
Release Date
1999
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM C799-12
Latest
ASTM C799-19
Scope

Uranyl nitrate solution is used as a feed material for conversion to the hexafluoride as well as for direct conversion to the oxide. In order to be suitable for this purpose, the material must meet certain criteria for uranium content, isotopic composition, acidity, radioactivity, and impurity content. These methods are designed to show whether a given material meets the specifications for these items described in Specification C 788.

3.1.1 An assay is performed to determine whether the material has the specified uranium content.

3.1.2 Determination of the isotopic content of the uranium is made to establish whether the effective fissile content is in accordance with the purchaserrsquo;specifications.

3.1.3 Acidity, organic content, and alpha, beta, and gamma activity are measured to establish that they do not exceed their maximum limits.

3.1.4 Impurity content is determined to ensure that the maximum concentration limit of certain impurity elements is not exceeded. Impurity concentrations are also required for calculation of the equivalent boron content (EBC), and the total equivalent boron content (TEBC).

1.1 These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade uranyl nitrate solution to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 5.

ASTM C799-99(2005) Referenced Document

  • ASTM C1219 Standard Test Methods for Arsenic in Uranium Hexafluoride
  • ASTM C1233 Standard Practice for Determining Equivalent Boron Contents of Nuclear Materials
  • ASTM C1254 Standard Test Method for Determination of Uranium in Mineral Acids by X-Ray Fluorescence
  • ASTM C1267 Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium*2022-07-01 Update
  • ASTM C1287 Standard Test Method for Determination of Impurities in Uranium Dioxide by Inductively Coupled Plasma Mass Spectrometry
  • ASTM C1295 Standard Test Method for Gamma Energy Emission from Fission Products in Uranium Hexafluoride
  • ASTM C1296 Standard Test Method for Determination of Sulfur in Uranium Oxides and Uranyl Nitrate Solutions by X-Ray Fluorescence (XRF)
  • ASTM C1380 Standard Test Method for Determination of Uranium Content and Isotopic Composition by Isotope Dilution Mass Spectrometry
  • ASTM C1413 Standard Test Method for Isotopic Analysis of Hydrolyzed Uranium Hexafluoride and Uranyl Nitrate Solutions by Thermal Ionization Mass Spectrometry
  • ASTM C696 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Uranium Dioxide Powders and Pellets
  • ASTM C761 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium Hexafluoride
  • ASTM C788 Standard Specification for Nuclear-Grade Uranyl Nitrate Solution
  • ASTM D1193 Standard Specification for Reagent Water
  • ASTM E12 
  • ASTM E60 Standard Practice for Analysis of Metals, Ores, and Related Materials by Molecular Absorption Spectrometry
  • ISO 7097 Determination of uranium in reactor fuel solutions and in uranium product solutions; Iron (II) sulfate reduction/potassium dichromate oxidation titrimetric method

ASTM C799-99(2005) history

  • 2019 ASTM C799-19 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Uranyl Nitrate Solutions
  • 2012 ASTM C799-12 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Uranyl Nitrate Solutions
  • 1999 ASTM C799-99(2005) Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Uranyl Nitrate Solutions
  • 1999 ASTM C799-99e1 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Uranyl Nitrate Solutions
Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Uranyl Nitrate Solutions



Copyright ©2024 All Rights Reserved