ASTM C114-22
Standard Test Methods for Chemical Analysis of Hydraulic Cement

Standard No.
ASTM C114-22
Release Date
2022
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM C114-23
Latest
ASTM C114-23
Scope
1.1 These test methods cover the chemical analyses of hydraulic cements. Any test methods of demonstrated acceptable precision and bias may be used for analysis of hydraulic cements, including analyses for referee and certification purposes, as explained in Section 4. Specific chemical test methods are provided for ease of reference for those desiring to use them. They are grouped as Reference Test Methods and Alternative Test Methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements. The alternative test methods generally provide individual determination of specific analytes and may be used alone or as alternates and determinations within the basic scheme at the option of the analyst and as indicated in the individual method. 1.2 Contents: Section Subject 2 Referenced Documents 4 Description of Referee Analyses 4.1 Referee Analyses 5 Qualification for Different Analyses 5.1 Certified Reference Materials 5.2 Requirements for Qualification Testing 5.3 Alternative Analyses 5.4 Performance Requirements for Rapid Test Methods 6 General 6.1 Interferences and Limitations 6.2 Apparatus and Materials 6.3 Reagents 6.4 Sample Preparation 6.5 General Procedures 6.6 Recommended Order for Reporting Analyses Reference Test Methods 7 Insoluble Residue 8 Silicon Dioxide 8.2 Cements with Insoluble Residue Less Than 1 % 8.3 Cements with Insoluble Residue Greater Than 1 % 9 Ammonium Hydroxide Group 10 Ferric Oxide 11 Phosphorus Pentoxide 12 Titanium Dioxide 13 Zinc Oxide 14 Aluminum Oxide 15 Calcium Oxide 16 Magnesium Oxide 17 Sulfur 17.1 Sulfur Trioxide 17.2 Sulfide 18 Loss On Ignition 18.1 Portland Cement 18.2 Portland Blast-Furnace Slag Cement and Slag Cement 19 Sodium and Potassium Oxides 19.1 Total Alkalis 19.2 Water-Soluble Alkalis 20 Manganic Oxide 21 Chloride 22 Chloroform-Soluble Organic Substances Alternative Test Methods 23 Calcium Oxide 24 Carbon Dioxide 25 Magnesium Oxide 26 Loss on Ignition 26.1 Portland Blast-Furnace Slag Cement and Slag Cement 27 Titanium Dioxide 28 Phosphorus Pentoxide 29 Manganic Oxide 30 Free Calcium Oxide Appendices Appendix X1 Example of Determination of Equivalence Point for the Chloride Determination Appendix X2 CO2 Determinations in Hydraulic Cements 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 These test methods are under the jurisdiction of ASTM Committee C01 on Cement and are the direct responsibility of Subcommittee C01.23 on Compositional Analysis. Current edition approved Dec. 15, 2022. Published December 2022. Originally approved in 1934. Last previous edition approved in 2018 as C114 – 18. DOI: 10.1520/C0114-22. *A Summary of Changes section appears at the end of this standard Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 2. Referenced Documents

ASTM C114-22 Referenced Document

  • ASTM C219 Standard Terminology Relating to Hydraulic and Other Inorganic Cements*2024-04-01 Update
  • ASTM C25 Standard Test Methods for Chemical Analysis of Limestone, Quicklime, and Hydrated Lime
  • ASTM E275 Standard Practice for Describing and Measuring Performance of Ultraviolet, Visible, and Near-Infrared Spectrophotometers
  • ASTM E29 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
  • ASTM E350 Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
  • ASTM E617 Standard Specification for Laboratory Weights And Precision Mass Standards
  • ASTM E832 Standard Specification for Laboratory Filter Papers

ASTM C114-22 history

  • 2023 ASTM C114-23 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2022 ASTM C114-22 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2018 ASTM C114-18 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2015 ASTM C114-15 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2013 ASTM C114-13 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2011 ASTM C114-11be1 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2011 ASTM C114-11b Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2011 ASTM C114-11a Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2011 ASTM C114-11 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2010 ASTM C114-10a Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2010 ASTM C114-10 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2009 ASTM C114-09b Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2009 ASTM C114-09a Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2009 ASTM C114-09 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2007 ASTM C114-07 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2006 ASTM C114-06e1 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2006 ASTM C114-06 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2005 ASTM C114-05 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2004 ASTM C114-04a Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2004 ASTM C114-04 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2003 ASTM C114-03 Standard Test Methods for Chemical Analysis of Hydraulic Cement
  • 2000 ASTM C114-00 Standard Test Methods for Chemical Analysis of Hydraulic Cement
Standard Test Methods for Chemical Analysis of Hydraulic Cement



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