1.1 This test method covers the determination of stable fission product 148 Nd in irradiated uranium (U) fuel (with initial plutonium (Pu) content from 0 to 50 %) as a measure of fuel burnup (1-3).2
1.2 It is possible to obtain additional information about the uranium and plutonium concentrations and isotopic abundances on the same sample taken for burnup analysis. If this additional information is desired, it can be obtained by precisely measuring the spike and sample volumes and following the instructions in Test Method E267.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM E321-20 Referenced Document
ASTM C1168 Standard Practice for Preparation and Dissolution of Plutonium Materials for Analysis
ASTM C1267 Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium*, 2022-07-01 Update
ASTM C1347 Standard Practice for Preparation and Dissolution of Uranium Materials for Analysis*, 2023-01-01 Update
ASTM C1411 Standard Practice for the Ion Exchange Separation of Uranium and Plutonium Prior to Isotopic Analysis
ASTM C1415 Standard Test Method for 238Pu Isotopic Abundance by Alpha Spectrometry
ASTM C1625 Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances by Thermal Ionization Mass Spectrometry
ASTM C1672 Standard Test Method for Determination of the Uranium, Plutonium or Americium Isotopic Composition or Concentration by the Total Evaporation Method Using a Thermal Ionization Mass Spectrometer*, 2024-01-26 Update
ASTM C1832 Standard Test Method for Determination of Uranium Isotopic Composition by Modified Total Evaporation (MTE) Method Using Thermal Ionization Mass Spectrometer*, 2023-01-01 Update
ASTM C1845 Standard Practice for The Separation of Lanthanide Elements from Uranium Matrices Using High Pressure Ion Chromatography (HPIC) for Isotopic Analyses by Inductively Coupled Plasma Mass Spectrometry (ICP-MS)*, 2024-04-21 Update
ASTM C859 Standard Terminology Relating to Nuclear Materials
ASTM D1193 Standard Specification for Reagent Water
ASTM E180 Standard Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals
ASTM E244 Test Method for Atom Percent Fission in Uranium and Plutonium Fuel (Mass Spectrometric Method) (Withdrawn 2001)*, 2021-03-02 Update
ASTM E267 Standard Test Method for Uranium and Plutonium Concentrations and Isotopic Abundances
ASTM E321-20 history
2020ASTM E321-20 Standard Test Method for Atom Percent Fission in Uranium and Plutonium Fuel (Neodymium-148 Method)
1996ASTM E321-96(2012) Standard Test Method for Atom Percent Fission in Uranium and Plutonium Fuel (Neodymium-148 Method)
1996ASTM E321-96(2005) Standard Test Method for Atom Percent Fission in Uranium and Plutonium Fuel (Neodymium-148 Method)
1996ASTM E321-96 Standard Test Method for Atom Percent Fission in Uranium and Plutonium Fuel (Neodymium-148 Method)