BS EN ISO 21814:2022
Fine ceramics (advanced ceramics, advanced technical ceramics). Methods for chemical analysis of aluminium nitride powders

Standard No.
BS EN ISO 21814:2022
Release Date
2023
Published By
British Standards Institution (BSI)
Status
Replace By
BS EN ISO 21814:2022(2023)
Latest
BS EN ISO 21814:2022(2023)
Scope
1   Scope This document specifies methods for the chemical analysis of fine aluminium nitride powders used as the raw material for fine ceramics. This document stipulates the determination methods of the aluminium, total nitrogen, boron, calcium, copper, iron, magnesium, manganese, molybdenum, nickel, potassium, silicon, sodium, titanium, tungsten, vanadium, zinc, zirconium, carbon, chlorine, fluorine, and oxygen contents in aluminium nitride powders. The aluminium content is determined by using either an acid pressure decomposition-CyDTA-zinc back titration method or an acid digestion-inductively coupled plasma-optical emission spectrometry (ICP-OES) method. The total nitrogen content is determined by using an acid pressure decomposition-distillation separation-acidimetric titration method, a direct decomposition-distillation separation-acidimetric titration method, or an inert gas fusion-thermal conductivity method. The boron, calcium, copper, iron, magnesium, manganese, molybdenum, nickel, potassium, silicon, sodium, titanium, tungsten, vanadium and zinc contents are determined by using an acid digestion-ICP-OES method or an acid pressure decomposition-ICP-OES method. The sodium and potassium contents are determined via an acid pressure decomposition-flame emission method or an acid pressure decomposition-atomic absorption spectrometry method. The oxygen content is determined by using an inert gas fusion-IR absorption spectrometry method, while that of carbon is determined via a combustion-IR absorption spectrometry method or a combustion-conductometry method. The chlorine and fluorine contents are determined by using a pyrohydrolysation method followed by ion chromatography or spectrophotometry.<...

BS EN ISO 21814:2022 history

  • 0000 BS EN ISO 21814:2022(2023)
  • 2023 BS EN ISO 21814:2022 Fine ceramics (advanced ceramics, advanced technical ceramics). Methods for chemical analysis of aluminium nitride powders



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