ASTM D8064-16 PDF

Scope: 1.1 This test method is based upon energy-dispersive X-ray Fluorescence (EDXRF) spectrometry using multiple monochromatic excitation beams for detection and quantification of selected heavy metal elements in soil and related solid waste. 1.2 This test method is also known as High Definition X-ray Fluorescence (HDXRF) or Multiple Monochromatic Beam EDXRF (MMB-EDXRF). 1.3 This test method is applicable to various soil matrices for the determination of Cr, Ni, As, Cd, Hg, and Pb in the range of 1 to 5000 mg/kg, as specified in Table 1 and determined by a ruggedness study using representative samples. The limit of detection (LOD) for each element is listed in Table 1. The LOD is estimated by measuring a SiO2 blank sample (see Table X1.1 in Appendix X1). 1.4 This test method is applicable to other elements: Sb, Cu, Se, Ag, Tl, Zn, Ba, Au, Co, V, Fe, Mn, Mo, K, Rb, Sn, Sr, and Ti. 1.5 X-ray Nomenclature—This standard names X-ray lines using the Siegbahn convention.2 1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D8064-16 Referenced Document

ASTM D4944 Standard Test Method for Field Determination of Water (Moisture) Content of Soil by the Calcium Carbide Gas Pressure Tester Method
ASTM D5283 Standard Practice for Generation of Environmental Data Related to Waste Management Activities: Quality Assurance and Quality Control Planning and Implementation
ASTM D5681 Standard Terminology for Waste and Waste Management
ASTM D5847 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D653 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM E1169 Standard Guide for Conducting Ruggedness Tests
ASTM E1727 Standard Practice for Field Collection of Soil Samples for Lead Determination by Atomic Spectrometry Techniques
ASTM E2554 Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques*， 2018-04-01 Update

2016 ASTM D8064-16 Standard Test Method for Elemental Analysis of Soil and Solid Waste by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry Using Multiple Monochromatic Excitation Beams