1.1 This guide covers and describes the factors that influence laboratory immersion corrosion tests, particularly mass loss tests. These factors include apparatus, sampling, test specimen, test conditions (test solution composition, temperature, gas sparging, fluid motion, solution volume, method of supporting test specimens, duration of test), methods of cleaning test specimens, interpretation of results, and calculation of corrosion rates. This guide also emphasizes the importance of recording all pertinent data and provides a checklist for reporting test data.
1.2 The specific evaluation of localized attack, environmentally assisted cracking, and effects of solution flow are not within the scope of this guide.
1.3 This guide is intended to be used by those designing laboratory immersion tests who may not be familiar with all of the variables to consider and the pitfalls that could be encountered when designing and conducting this kind of testing. It should be used as a reference to ensure that the test will allow generation of data relevant to the application with the minimum of interferences.
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
ASTM G31-12a Referenced Document
ASTM A262 Standard Practices for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels
ASTM D1193 Standard Specification for Reagent Water
ASTM E300 Standard Practice for Sampling Industrial Chemicals
ASTM E8 Standard Test Methods for Tension Testing of Metallic Materials
ASTM G1 Standard Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens
ASTM G107 Standard Guide for Formats for Collection and Compilation of Corrosion Data for Metals for Computerized Database Input
ASTM G108 Standard Test Method for Electrochemical Reactivation (EPR) for Detecting Sensitization of AISI Type 304 and 304L Stainless Steels
ASTM G110 Standard Practice for Evaluating Intergranular Corrosion Resistance of Heat Treatable Aluminum Alloys by Immersion in Sodium Chloride + Hydrogen Peroxide Solution
ASTM G112 Standard Guide for Conducting Exfoliation Corrosion Tests in Aluminum Alloys
ASTM G116 Standard Practice for Conducting Wire-on-Bolt Test for Atmospheric Galvanic Corrosion
ASTM G135 Standard Guide for Computerized Exchange of Corrosion Data for Metals
ASTM G170 Standard Guide for Evaluating and Qualifying Oilfield and Refinery Corrosion Inhibitors in the Laboratory
ASTM G184 Standard Practice for Evaluating and Qualifying Oil Field and Refinery Corrosion Inhibitors Using Rotating Cage
ASTM G185 Standard Practice for Evaluating and Qualifying Oil Field and Refinery Corrosion Inhibitors Using the Rotating Cylinder Electrode
ASTM G193 Standard Terminology and Acronyms Relating to Corrosion
ASTM G28 Standard Test Methods of Detecting Susceptibility to Intergranular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys
ASTM G34 Standard Test Method for Exfoliation Corrosion Susceptibility in 2XXX and 7XXX Series Aluminum Alloys (EXCO Test)
ASTM G46 Standard Guide for Examination and Evaluation of Pitting Corrosion
ASTM G48 Standard Test Methods for Pitting and Crevice Corrosion Resistance of Stainless Steels and Related Alloys by Use of Ferric Chloride Solution
ASTM G66 Standard Test Method for Visual Assessment of Exfoliation Corrosion Susceptibility of 5XXX Series Aluminum Alloys (ASSET Test)
ASTM G67 Standard Test Method for Determining the Susceptibility to Intergranular Corrosion of 5XXX Series Aluminum Alloys by Mass Loss After Exposure to Nitric Acid (NAMLT Test)
ASTM G71 Standard Guide for Conducting and Evaluating Galvanic Corrosion Tests in Electrolytes
ASTM G78 Standard Guide for Crevice Corrosion Testing of Iron-Base and Nickel-Base Stainless Alloys in Seawater and Other Chloride-Containing Aqueous Environments
ASTM G82 Standard Guide for Development and Use of a Galvanic Series for Predicting Galvanic Corrosion Performance*, 2024-04-21 Update
ISO 11463 Corrosion of metals and alloys — Guidelines for the evaluation of pitting corrosion
ISO 11845 Corrosion of metals and alloys — General principles for corrosion testing
ISO 11846 Corrosion of metals and alloys - Determination of resistance to intergranular corrosion of solution heat-treatable aluminium alloys
ISO 11881 Corrosion of metals and alloys - Exfoliation corrosion testing of aluminium alloys; Technical Corrigendum 1
ISO 3651-1 Determination of resistance to intergranular corrosion of stainless steels - Part 1: Austenitic and ferritic-austenitic (duplex) stainless steels - Corrosion test in nitric acid medium by measurement of loss in mass (Huey test)
ISO 3651-2 Determination of resistance to intergranular corrosion of stainless steels - Part 2: Ferritic, austenitic and ferritic-austenitic (duplex) stainless steels - Corrosion test in media containing sulfuric acid
ISO 6509 Corrosion of metals and alloys; Determination of dezincification resistance of brass